National foreword

This British Standard is the UK implementation of EN ISO 19628:2024. It is identical to ISO 19628:2024. It supersedes BS EN ISO 19628:2021, which is withdrawn.

The UK participation in its preparation was entrusted to Technical Committee RPI/13, Advanced technical ceramics.

A list of organizations represented on this committee can be obtained on request to its committee manager.

Contractual and legal considerations

This publication has been prepared in good faith, however no representation, warranty, assurance or undertaking (express or implied) is or will be made, and no responsibility or liability is or will be accepted by BSI in relation to the adequacy, accuracy, completeness or reasonableness of this publication. All and any such responsibility and liability is expressly disclaimed to the full extent permitted by the law.

This publication is provided as is, and is to be used at the recipient’s own risk.

The recipient is advised to consider seeking professional guidance with respect to its use of this publication.

This publication is not intended to constitute a contract. Users are responsible for its correct application.

Compliance with a British Standard cannot confer immunity from legal obligations.

This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 November 2024.

This European Standard was approved by CEN on 21 July 2024.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czechia, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and United Kingdom.

European foreword

This document (EN ISO 19628:2024) has been prepared by Technical Committee ISO/TC 206 "Fine ceramics" in collaboration with Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by DIN.

This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2025, and conflicting national standards shall be withdrawn at the latest by May 2025.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN ISO 19628:2021.

Any feedback and questions on this document should be directed to the users’ national standards body/national committee. A complete listing of these bodies can be found on the CEN website.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the United Kingdom.

Endorsement notice

The text of ISO 19628:2024 has been approved by CEN as EN ISO 19628:2024 without any modification.

Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types of ISO document should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).

ISO draws attention to the possibility that the implementation of this document may involve the use of (a) patent(s). ISO takes no position concerning the evidence, validity or applicability of any claimed patent rights in respect thereof. As of the date of publication of this document, ISO had not received notice of (a) patent(s) which may be required to implement this document. However, implementers are cautioned that this may not represent the latest information, which may be obtained from the patent database available at www.iso.org/patents. ISO shall not be held responsible for identifying any or all such patent rights.

Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.

For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISO's adherence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.

This document was prepared by Technical Committee ISO/TC 206, Fine ceramics, in collaboration with the European Committee for Standardization (CEN) Technical Committee CEN/TC 184, Advanced technical ceramics, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienna Agreement).

This second edition cancels and replaces the first edition (ISO 19268:2017), which has been technically revised.

The main changes are as follows:

revised scope to extend the maximum temperature of use of Method A to 3 000 K;
revised Clause 4 by introducing the possibility to apply the drop calorimetry method for temperatures T1 > T2 (conventional drop calorimetry);
relevant specifications added concerning the containers and thermometers to be used;
description of in-situ calibration methods of the calorimeter and thermometers;
addition of a paragraph dealing with the determination of specific heat capacity at given temperatures from measurements performed by drop calorimetry;
updated list of references in the Bibliography.

Any feedback or questions on this document should be directed to the user’s national standards body. A complete listing of these bodies can be found at www.iso.org/members.html.

1 Scope

This document specifies two methods for the determination of the specific heat capacity of ceramic matrix composites with continuous reinforcements (1D, 2D, 3D).

Unidirectional (1D), bi-directional (2D) and tridirectional (XD, with 2 < X ≤ 3).

The two methods are:

method A: drop calorimetry;
method B: differential scanning calorimetry.

The two methods are applicable from ambient temperature up to a maximum temperature that is method dependent: method A can be used up to 3 000 K, while method B is limited to 1 900 K.

2 Normative references

3 Terms and definitions

4 Method A – drop calorimetry

4.1 Principle

4.2 Apparatus

4.3 Standard reference materials

4.4 Containers

4.5 Test specimens

4.6 Calibration of the calorimeter

4.7 Test procedures

4.8 Calculations

5 Method B – differential scanning calorimetry

5.1 Principle

5.2 Apparatus

5.3 Standard reference materials, SRM

5.4 Test specimens

5.5 Temperature calibration

5.6 Test procedure for the determination of C_p

5.7 Calculation of results

6 Test report

Bibliography

BS EN ISO 19628:2024

Fine ceramics (advanced ceramics, advanced technical ceramics). Thermophysical properties of ceramic composites. Determination of specific heat capacity

Current

Published:

30 Nov 2024