1 Scope
This document specifies methods for calculating the resin, fibre and void contents of a carbon-fibre-reinforced composite from the densities of the resin, the fibre
and the composite and the mass of fibre in the composite (using method A), for calculating
the fibre content from the thickness of the composite (using method B), and for calculating
the fibre content by volume and areal void content through microscopic analysis (using method C).
Method A specifies three different resin removal procedures for the determination
of the mass of fibre in the composite (viz a combustion procedure, a procedure by
digestion in nitric acid and a procedure by digestion in a mixture of sulfuric acid
and hydrogen peroxide). The selection of the procedure to be used is made by considering
the combustibility of the resin used in the composite, its ability to decompose and
the type of resin concerned. Method A is only of limited applicability when filled
resins are present that can prevent complete dissolution and/or combustibility of
the resin.
Method B (thickness measurement method) is only applicable to composites moulded from
prepregs of known fibre mass per unit area.
Method C (microscopic method) is only applicable to carbon-fibre-reinforced composites
with unidirectional, orthogonal and multidirectional laminates. It can also be used
as reference for determination of the areal void content and fibre volume content of aramid- or glass-fibre-reinforced plastics, but is not
applicable to fabric reinforced composites.